Spectrometric Identification of Organic Compounds, 8ed (An Indian Adaptation)

Robert M. Silverstein , Francis X. Webster , David J. Kiemle , David L. Bryce, Wiley Editorial Team

ISBN: 9789354642296

INR 879

Description

The Indian Adaptation of Spectrometric Identification of Organic Compounds, eighth edition of the book is reorganized, enhanced, and updated to offer complete coverage of Indian curriculum. Almost all spectroscopic techniques include updates in theory, instrumentation, and characterization of group absorptions UV-Visible Spectroscopy is now included as a part of the book. Chapter on Two-Dimensional NMR Spectroscopy is reorganized to explain 2D NMR techniques first with examples of simple molecules and then applied to analyze more complex molecules.

Preface to the Adapted Edition

Preface to Eighth Edition

Preface to First Edition

 

Chapter 1 Ultraviolet-Visible Spectroscopy

1.1 Introduction

1.2 Theory

1.3 Instrumentation

1.4 Characteristic Absorption of Organic Compounds

 

Chapter 2 Mass Spectrometry

2.1 Introduction

2.2 Instrumentation

2.3 Ionization Methods

2.4 Mass Analyzers

2.5 Interpretation of EI Mass Spectra

2.6 Mass Spectra of Some Chemical Classes

2.7 Other Applications of Mass Spectrometry

 

Chapter 3 Infrared Spectroscopy

3.1 Introduction

3.2 Theory

3.3 Instrumentation

3.4 Sample Handling

3.5 Interpretation of Spectra

3.6 Characteristic Group Absorptions of Organic Molecules

 

Chapter 4 Proton (1H) Magnetic Resonance Spectroscopy

4.4 Chemical Shift

4.5 Spin–spin Coupling, Multiplets, and Spin Systems

4.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms: Exchangeable Protons

4.7 Coupling of Protons to Other Important Nuclei (19F, D (2H), 31P, 29Si, and 13C)

4.8 Chemical Equivalence

4.9 Magnetic Equivalence

4.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants

4.11 Weakly and Strongly Coupled Systems: Virtual Coupling

4.12 Chirality

4.13 Magnitude of Vicinal and Geminal Coupling Constants

4.14 Long-range Coupling

4.15 Simplification of Complex NMR Spectra

4.16 Nuclear Overhauser Effect

4.17 Solid-State NMR

4.18 Conclusion

 

Chapter 5 Carbon-13 NMR Spectroscopy*

5.1 Introduction

5.2 Theory

5.3 Interpretation of a Simple 13C NMR Spectrum: Diethyl Phthalate

5.4 Quantitative 13C Analysis

5.5 Chemical Equivalence

5.6 Dept

5.7 Chemical Classes and Chemical Shifts

 

Chapter 6 Two-dimensional NMR Spectroscopy

6.1 Introduction

6.2 Theory

6.3 Homonuclear Correlation Techniques

6.4 Heteronuclear Correlation Techniques

6.5 Ipsenol

6.6 Caryophyllene Oxide

6.7 Lactose

6.8 VGSE

 

Chapter 7 Multinuclear Magnetic Resonance Spectroscopy

7.1 Introduction and General Considerations

7.2 15N Nuclear Magnetic Resonance

7.3 19F Nuclear Magnetic Resonance

7.4 29Si Nuclear Magnetic Resonance

7.5 31P Nuclear Magnetic Resonance

7.6 Conclusions

 

Chapter 8 Solved Problems

8.1 Introduction

8.2 Solved Problems

 

Chapter 9 Assigned Problems

9.1 Introduction

9.2 Structure Elucidation of Simple Molecules Using IR/MS/1H NMR and 13C/DEPT Spectral Data

9.3 Structure Elucidation of Molecules Using I/MS/ 1H NMR and 13C/DEPT Spectra

9.4 Structure Elucidation of Molecules Using IR/MS/ 1H NMR and 13C/DEPT and 2D NMR

9.5 Additional Spectra and Exercises

 

References

Index

 

 

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